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e-Pub 1993

Subsequently, the peptides were separated on a Pepmap100 RSLC C18 column (2.0 m, 75 m 150 mm, Thermo Fisher Scientific) using a multistep gradient of 2% to 40% acetonitrile with 0.1% formic acid over a period of 150 min

Am J Clin Oncol 43(4):231-235, 2020

However, from what we know anecdotally and from limited studies, people have used MK-677 continuously for up to 6 months without any noticeable side effects, sticking to around 30 mg per day